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HRID735038

反应详情

EQUATION

反应方程式

HRID 735038 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)C#Cc1ccc(Cl)cc1Cl
HCID228509

3-(2,4-dichlorophenyl)prop-2-ynoic acid

C9H4Cl2O2

结构：CCO.ClCCl.N
HCID22609213

未命名化合物

结构：CCN(CC)C(C)COc1ccc(N)cc1
HCID68816089

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CC)C(C)COc1ccc(NC(=O)C#Cc2ccc(Cl)cc2Cl)cc1
HCID68816600

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 3.4.c. from 4-(2-diethylaminopropoxy)phenylamine and (2,4-dichlorophenyl)propynoic acid. Yield: 0.41 g (65.2% of theory); melting point: 70° C.-72° C.; C22H24Cl2N2O2 (M=419.35); calc.: molecular ion peak (M+H)+: 419/421/423; found: molecular ion peak (M+H)+: 419/421/423; Rf value: 0.4 (silica gel, dichloromethane/ethanol/ammonia (5:1:0.01)).

WORKUP

后处理

  1. customPrepared analogously to Example 3.4.c