反应详情

Prepared analogously to Example 3.1.e. from [(E)-3-(4′-chlorobiphenyl-4-yl)acrylic acid and 4-piperidin-1-ylmethylphenylamine. Yield: 0.57 g (62.9% of theory); melting point: 265° C.-270° C.; C27H27ClN2O (M=430.98); calc.: molecular ion peak (M+H)+: 431/433; found: molecular ion peak (M+H)+: 431/433; Rf value: 0.31 (silica gel, dichloromethane/methanol (90:10)).

1. customPrepared analogously to Example 3.1.e