HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia methanol dichloromethane → HCID 57845728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia methanol dichloromethane | HCID 21584172 | — |
| Reactant | HCID 68817360 | HCID 68817360 | — |
| Product | HCID 57845728 | HCID 57845728 | — |
Reaction Steps
Prepared analogously to Example 3.4.b. from 2.3-dibromo-3-(4′-chlorobiphenyl-4-yl)-N-(4-piperidin-1-ylmethylphenyl)propionamide. Yield: 26 mg (23.9% of theory); C27H25ClN2O (M=428.96); calc.: molecular ion peak (M+H)+: 429/431; found: molecular ion peak (M+H)+: 429/431; Rf value: 0.42 (silica gel, dichloromethane/methanol/ammonia (90:10:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-7ff5a2da50294a7c9eddf2db90a77492 |
| Source note | uspto-grants-2009_09 |