反应详情

Prepared analogously to Example 3.7.c. from (4′-chlorobiphenyl-4-yl)propynoic acid and 3-chloro-4-piperidin-1-ylmethylphenylamine. Yield: 0.1 g (22% of theory); melting point: 277° C.-281° C.; C27H24Cl2N2 0 (M=463.4); calc.: molecular ion peak (M+H)+: 463/5/7 (Cl2); found: molecular ion peak (M+H)+: 463/5/7 (Cl2); Rf value: 0.50 (silica gel, dichloromethane/methanol (90:10)).

1. customPrepared analogously to Example 3.7.c