huagongshe.com
HRID735059

反应详情

EQUATION

反应方程式

HRID 735059 的结构方程式

REACTANTS

反应物

3
结构：Nc1ccc(CN2CCCCC2)cc1
HCID846150

4-(piperidin-1-ylmethyl)aniline

C12H18N2

结构：CO.ClCCl.N
HCID21584172

未命名化合物

结构：O=C(O)C#Cc1ccc(-c2ccc(Cl)cc2)cn1
HCID68816808

未命名化合物

PRODUCTS

生成物

1
结构：O=C(C#Cc1ccc(-c2ccc(Cl)cc2)cn1)Nc1ccc(CN2CCCCC2)cc1
HCID57845733

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 2.3.f. from [5-(4-chlorophenyl)pyridin-2-yl]propynoic acid and 4-piperidin-1-ylmethylphenylamine. Yield: 0.2 g (48% of theory); C26H24ClN3O (M=429.95); calc.: molecular ion peak (M+H)+: 430/432; found: molecular ion peak (M+H)+: 430/432; Rf value: 0.4 (silica gel, dichloromethane/methanol/ammonia (90:10:0.1)).

WORKUP

后处理

  1. customPrepared analogously to Example 2.3.f