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HRID735065

反应详情

EQUATION

反应方程式

HRID 735065 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)C#Cc1ccc(Cl)cc1Cl
HCID228509

3-(2,4-dichlorophenyl)prop-2-ynoic acid

C9H4Cl2O2

结构：CCN(CC)CCc1ccc(N)cc1
HCID22569266

未命名化合物

结构：CCO.ClCCl.N
HCID22609213

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CC)CCc1ccc(NC(=O)C#Cc2ccc(Cl)cc2Cl)cc1.Cl
HCID68820353

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 2.3.f. from 4-(2-diethylaminoethyl)phenylamine and (2,4-dichlorophenyl)propynoic acid. Yield: 0.3 g (47% of theory); melting point: 204° C.-208° C.; C21H22Cl2N2O (M=425.78); calc.: molecular ion peak (M+H)+: 389/391/393; found: molecular ion peak (M+H)+: 389/391/393; Rf value: 0.6 (silica gel, dichloromethane/ethanol/ammonia (5:1:0.01)).

WORKUP

后处理

  1. customPrepared analogously to Example 2.3.f