HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2,4-dichlorophenyl)prop-2-ynoic acid → HCID 68820353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2,4-dichlorophenyl)prop-2-ynoic acid | HCID 228509 | — |
| Reactant | 4-[2-(Diethylamino)ethyl]aniline | HCID 22569266 | — |
| Reactant | HCID 22609213 | HCID 22609213 | — |
| Product | HCID 68820353 | HCID 68820353 | — |
Reaction Steps
Prepared analogously to Example 2.3.f. from 4-(2-diethylaminoethyl)phenylamine and (2,4-dichlorophenyl)propynoic acid. Yield: 0.3 g (47% of theory); melting point: 204° C.-208° C.; C21H22Cl2N2O (M=425.78); calc.: molecular ion peak (M+H)+: 389/391/393; found: molecular ion peak (M+H)+: 389/391/393; Rf value: 0.6 (silica gel, dichloromethane/ethanol/ammonia (5:1:0.01)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-c5738f73bd5f42b6aa20953397de0e4d |
| Source note | uspto-grants-2009_09 |