HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(diethylaminomethyl)aniline → HCID 57845846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(diethylaminomethyl)aniline | HCID 236803 | — |
| Reactant | (2-Chloro-4-trifluoromethylphenyl)propynoic acid | HCID 68817422 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 57845846 | HCID 57845846 | — |
Reaction Steps
Prepared analogously to Example 2.3.f. from 4-diethylaminomethylphenylamine and (2-chloro-4-trifluoromethylphenyl)propynoic acid. Yield: 72 mg (59% of theory); C21H20ClF3N2O (M=408.85); calc.: molecular ion peak (M+H)+: 409/411; found: molecular ion peak (M+H)+: 409/411; Rf value: 0.35 (silica gel, dichloromethane/methanol (9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-98669d61f45e45bab239d74510b45566 |
| Source note | uspto-grants-2009_09 |