HRID735082
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Prepared analogously to Example 2.3.f. from pyridin-2-ylpropynoic acid and [2-(2-chloro-4-aminophenoxy)ethyl]diethylamine. Yield: 0.37 g (53.3% of theory); C20H22ClN3O2*HCl (M=408.33); calc.: molecular ion peak (M+H)+: 372/374; found: molecular ion peak (M+H)+: 372/374; Rf value: 0.5 (silica gel, dichloromethane/methanol/ammonia (9:1:0.1)).
WORKUP
后处理
- customPrepared analogously to Example 2.3.f