Ammonia methanol dichloromethane → HCID 68817646, compound

Participants

Reaction Steps

Prepared analogously to Example 3.1.b. from [2-(2-chloro-4-nitrophenoxy)propyl]diethylamine in methanol in a reaction time of 8 hours. Yield: 6.7 g (93.5% of theory); C13H21ClN2O (M=256.77); calc.: molecular ion peak (M+H)+: 257/259; found: molecular ion peak (M+H)+: 257/259; Rf value: 0.4 (silica gel, dichloromethane/methanol/ammonia (50:10:0.1)).

Provenance & Evidence