HRID735092

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID21226129

未命名化合物

HCID68816613

[2-(3-Chloro-4-nitrophenoxy)ethyl]diethylamine

C12H17ClN2O3

PRODUCTS

生成物

HCID57082476

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Prepared analogously to Example 3.1.b. from [2-(3-chloro-4-nitrophenoxy)ethyl]diethylamine in ethyl acetate. Yield: 1.05 g (95.4% of theory); C12H19ClN2O (M=242.75); calc.: molecular ion peak (M+H)+: 243/245; found: molecular ion peak (M+H)+: 243/245; Rf value: 0.41 (silica gel, dichloromethane/methanol (90:10)).

WORKUP

后处理

customPrepared analogously to Example 3.1.b