HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane methanol → [2-(3-Chloro-4-aminophenoxy)ethyl]diethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Reactant | [2-(3-Chloro-4-nitrophenoxy)ethyl]diethylamine | HCID 68816613 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | [2-(3-Chloro-4-aminophenoxy)ethyl]diethylamine | HCID 57082476 | — |
Reaction Steps
Prepared analogously to Example 3.1.b. from [2-(3-chloro-4-nitrophenoxy)ethyl]diethylamine in ethyl acetate. Yield: 1.05 g (95.4% of theory); C12H19ClN2O (M=242.75); calc.: molecular ion peak (M+H)+: 243/245; found: molecular ion peak (M+H)+: 243/245; Rf value: 0.41 (silica gel, dichloromethane/methanol (90:10)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-df9a410578e54743acc37b864927a314 |
| Source note | uspto-grants-2009_09 |