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HRID735103

反应详情

EQUATION

反应方程式

HRID 735103 的结构方程式

REACTANTS

反应物

2
结构：CO.ClCCl.N
HCID21584172

未命名化合物

结构：CCOC(=O)c1cc([N+](=O)[O-])ccc1OCCN(CC)CC
HCID57632929

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1cc(N)ccc1OCCN(CC)CC
HCID57632512

Ethyl 5-amino-2-[2-(diethylamino)ethoxy]benzoate

C15H24N2O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Prepared analogously to Example 3.1.b. from 0.30 g ethyl 2-(2-diethylaminoethoxy)-5-nitrobenzoate in ethyl acetate. Yield: 0.27 g (100% of theory); C15H24N2O3 (M=280.37); calc.: molecular ion peak (M+H)+: 281; found: molecular ion peak (M+H)+: 281; Rf value: 0.40 (silica gel, dichloromethane/methanol/ammonia (39:1:0.1)).

WORKUP

后处理

  1. customPrepared analogously to Example 3.1.b