HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylethanolamine → [2-(2-Bromo-4-nitrophenoxy)ethyl]diethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylethanolamine | HCID 7497 | — |
| Reactant | 2-Bromo-1-fluoro-4-nitrobenzene | HCID 69699 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | [2-(2-Bromo-4-nitrophenoxy)ethyl]diethylamine | HCID 68817905 | — |
Reaction Steps
Prepared analogously to Example 4.13.a. starting from 0.66 g (2.00 mmol) of 2-bromo-1-fluoro-4-nitrobenzene and 0.40 mL (3.00 mmol) of 2-diethylaminoethanol. Yield: 0.95 g (100% of theory); C12H17BrN2O3 (M=317.185); calc.: molecular ion peak (M+H)+: 317/319; found: molecular ion peak (M+H)+: 317/319; Rf value: 0.50 (silica gel, dichloromethane/methanol (9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-f278ac7c37944d6b8ea9fef903677cc4 |
| Source note | uspto-grants-2009_09 |