HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → 2-Chloro-N,N-diethyl-4-nitrobenzeneacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | (2-Chloro-4-nitrophenyl)acetic acid chloride | HCID 85969188 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-Chloro-N,N-diethyl-4-nitrobenzeneacetamide | HCID 68819533 | — |
Reaction Steps
Prepared analogously to Example 4.1.d. from (2-chloro-4-nitrophenyl)acetic acid chloride and diethylamine in ethyl acetate. Yield: 3.7 g (100% of theory); C12H15ClN2O3 (M=270.71); calc.: molecular ion peak (M+H)+: 271/273; found: molecular ion peak (M+H)+: 271/273; Rf value: 0.45 (silica gel, petroleum ether/ethyl acetate (1:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-4a3a17a439db4e02aacce54c1f070d6c |
| Source note | uspto-grants-2009_09 |