HRID735121

反应详情

EQUATION

反应方程式

HRID 735121 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Prepared analogously to Example 4.1.d. from (2-chloro-4-nitrophenyl)acetic acid chloride and diethylamine in ethyl acetate. Yield: 3.7 g (100% of theory); C12H15ClN2O3 (M=270.71); calc.: molecular ion peak (M+H)+: 271/273; found: molecular ion peak (M+H)+: 271/273; Rf value: 0.45 (silica gel, petroleum ether/ethyl acetate (1:1)).

WORKUP

后处理

  1. customPrepared analogously to Example 4.1.d