HRID735123
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Prepared analogously to Example 2.3.f. from (2-chloro-4-trifluoromethylphenyl)propynoic acid and 3-chloro-4-[2-(4-methylpiperidin-1-yl)ethyl]phenylamine. Yield: 0.21 g (45.3% of theory); C24H23Cl2F3N2O (M=483.36); calc.: molecular ion peak (M+H)+: 483/485/487; found: molecular ion peak (M+H)+: 483/485/487; Rf value: 0.65 (Alox, petroleum ether/ethyl acetate (1:1)).
WORKUP
后处理
- customPrepared analogously to Example 2.3.f