HRID735127
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
PROCEDURE
实验过程
Prepared analogously to Example 2.3.f. from (2-chloro-4-trifluoromethylphenyl)propynoic acid and 3-chloro-4-[2-(cyclopropylmethylamino)ethyl]phenylamine. Yield: 15 mg (3.4% of theory); C22H19Cl2F3N2O (M=455.31); calc.: molecular ion peak (M+H)+: 455/457/459; found: molecular ion peak (M+H)+: 455/457/459; Rf value: 0.3 (Alox, petroleum ether/ethyl acetate (3:1)).
WORKUP
后处理
- customPrepared analogously to Example 2.3.f