HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68816995, compound → HCID 68817874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68816995 | HCID 68816995 | — |
| Reactant | (2-Chloro-4-trifluoromethylphenyl)propynoic acid | HCID 68817422 | — |
| Product | HCID 68817874 | HCID 68817874 | — |
Reaction Steps
Prepared analogously to Example 2.3.f. from (2-chloro-4-trifluoromethylphenyl)propynoic acid and 3-chloro-4-[2-(cyclopropylmethylamino)ethyl]phenylamine. Yield: 15 mg (3.4% of theory); C22H19Cl2F3N2O (M=455.31); calc.: molecular ion peak (M+H)+: 455/457/459; found: molecular ion peak (M+H)+: 455/457/459; Rf value: 0.3 (Alox, petroleum ether/ethyl acetate (3:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-3800944a4d1344709868d58623a5e55b |
| Source note | uspto-grants-2009_09 |