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HRID735128

反应详情

EQUATION

反应方程式

HRID 735128 的结构方程式

REACTANTS

反应物

2
结构：CC1CCNCC1
HCID69381

Piperidine, 4-methyl-

C6H13N

结构：COc1cc([N+](=O)[O-])ccc1OCCBr
HCID12937254

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc([N+](=O)[O-])ccc1OCCN1CCC(C)CC1
HCID68818421

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.ClCCl
溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 1.1 C. from 1-(2-bromoethoxy)-2-methoxy-4-nitrobenzene and 4-methylpiperidine. Yield: 0.7 g (88.2% of theory); C15H22N2O4 (M=294.35); calc.: molecular ion peak (M+H)+: 295; found: molecular ion peak (M+H)+: 295; Rf value: 0.5 (silica gel, dichloromethane/methanol (9:1)).

WORKUP

后处理

  1. customPrepared analogously to Example 1.1 C