HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68817390, compound → HCID 68817651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68817390 | HCID 68817390 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 68817651 | HCID 68817651 | — |
Reaction Steps
Prepared analogously to Example 3.1.b. from {(S)-1-[2-(2-methoxy-4-nitrophenoxy)ethyl]pyrrolidin-2-yl}methanol. Yield: 0.15 g (83.4% of theory); C14H22N2O3 (M=266.34); calc.: molecular ion peak (M+H)+: 267; found: molecular ion peak (M+H)+: 267; Rf value: 0.15 (silica gel, dichloromethane/methanol 9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-de6479134b0e43f39a1b24253bd637e9 |
| Source note | uspto-grants-2009_09 |