反应详情

Prepared analogously to Example 3.1.b. from 1.4 g (2.77 mmol) of 2-[2-(2-methoxy-4-nitrophenoxy)ethyl]-1,2,3,4-tetrahydroisoquinoline (65%). Yield: 1.2 g (94% of theory); C18H22N2O2 (M=298.38); calc.: molecular ion peak (M+H)+: 299; found: molecular ion peak (M+H)+: 299; Rf value: 0.5 (silica gel, dichloromethane/methanol (9:1)).

1. customPrepared analogously to Example 3.1.b