HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidinecarboxamide → HCID 68818347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidinecarboxamide | HCID 3772 | — |
| Reactant | 1-(2-Bromoethoxy)2-methoxy-4-nitrobenzene | HCID 12937254 | — |
| Reactant | Ammonia methanol dichloromethane | HCID 21584172 | — |
| Product | HCID 68818347 | HCID 68818347 | — |
Reaction Steps
Prepared analogously to Example 1.1.c. from 1 g (3.622 mmol) of 1-(2-bromoethoxy)-2-methoxy-4-nitrobenzene and 1.4 g (10.87 mmol) of piperidine-4-carboxylic acid amide. Yield: 1.05 g (90% of theory); C15H21N3O5 (M=323.34); calc.: molecular ion peak (M+H)+: 324; found: molecular ion peak (M+H)+: 324; Rf value: 0.4 (silica gel, dichloromethane/methanol/ammonia (9:1:0.1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-c7e245ed313f4ce4ad52c78f2b07e0d9 |
| Source note | uspto-grants-2009_09 |