Ammonia methanol dichloromethane → HCID 68817417, compound

Participants

Reaction Steps

Prepared analogously to Example 3.1.b. from 1 g (3.1 mmol) of 1-[2-(2-methoxy-4-nitrophenoxy)ethyl]piperidine-4-carboxylic acid amide. Yield: 0.8 g (88% of theory); C15H23N3O3 (M=298.38); calc.: molecular ion peak (M+H)+: 294; found: molecular ion peak (M+H)+: 294; Rf value: 0.3 (silica gel, dichloromethane/methanol/ammonia (9:1:0.1)).

Provenance & Evidence