HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21101391, compound → HCID 68816035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21101391 | HCID 21101391 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 68816035 | HCID 68816035 | — |
Reaction Steps
Prepared analogously to Example 3.1.b. from 0.84 g (2.72 mmol) of 1-[2-(2-methoxy-4-nitrophenoxy)ethyl]-2,6-dimethylpiperidine. Yield: 0.65 g (86% of theory); C16H26N2O2 (M=278.39); calc.: molecular ion peak (M+H)+: 279; found: molecular ion peak (M+H)+: 279; Rf value: 0.1 (silica gel, dichloromethane/methanol (9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-8dfaad4764ed4969af08a4f56a73a636 |
| Source note | uspto-grants-2009_09 |