HRID735160
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Prepared analogously to Example 2.3.f. from (3-bromobiphenyl-4-yl)propynoic acid and 3-chloro-4-(2-diethylaminoethyl)phenylamine. Yield: 95 mg (23.8% of theory); C27H26BrClN2O*HCl (M=546.32); calc.: molecular ion peak (M+H)+: 509/11/13; found: molecular ion peak (M+H)+: 509/11/13; Rf value: 0.3 (silica gel, dichloromethane/methanol (90:10)).
WORKUP
后处理
- customPrepared analogously to Example 2.3.f