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HRID735168

反应详情

EQUATION

反应方程式

HRID 735168 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(-c2ccc(Cl)cc2)cc1
HCID8675

4-Amino-4'-chlorobiphenyl

C12H10ClN

结构：COC(OC)c1ccc(/C=C/C(=O)O)cc1
HCID57845776

未命名化合物

PRODUCTS

生成物

1
结构：COC(OC)c1ccc(/C=C/C(=O)Nc2ccc(-c3ccc(Cl)cc3)cc2)cc1
HCID68819697

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO.ClCCl
溶剂HCID21584144

Dichloromethane ethanol

C3H8Cl2O

PROCEDURE

实验过程

Prepared analogously to Example 3.1.e. from (E)-3-(4-dimethoxymethylphenyl)acrylic acid and 4′-chlorobiphenyl-4-ylamine. Yield: 9.8 g, C24H22ClNO3 (M=407.90); calc.: molecular ion peak (M+H)+: 408/410; found: molecular ion peak (M+H)+: 408/410; Rf value: 0.3 (silica gel, dichloromethane/ethanol (20:1)).

WORKUP

后处理

  1. customPrepared analogously to Example 3.1.e