HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-4'-chlorodiphenyl → (E)-N-(4'-chlorobiphenyl-4-yl)-3-(4-dimethoxymethylphenyl)acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-4'-chlorodiphenyl | HCID 8675 | — |
| Reactant | (E)-3-(4-dimethoxymethylphenyl)acrylic Acid | HCID 57845776 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | (E)-N-(4'-chlorobiphenyl-4-yl)-3-(4-dimethoxymethylphenyl)acrylamide | HCID 68819697 | — |
Reaction Steps
Prepared analogously to Example 3.1.e. from (E)-3-(4-dimethoxymethylphenyl)acrylic acid and 4′-chlorobiphenyl-4-ylamine. Yield: 9.8 g, C24H22ClNO3 (M=407.90); calc.: molecular ion peak (M+H)+: 408/410; found: molecular ion peak (M+H)+: 408/410; Rf value: 0.3 (silica gel, dichloromethane/ethanol (20:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-2e3a82b7a46c4169b7cd17176accc2dd |
| Source note | uspto-grants-2009_09 |