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HRID735173

反应详情

EQUATION

反应方程式

HRID 735173 的结构方程式

REACTANTS

反应物

2
结构：C[C@@H]1CNC[C@H](C)C1
HCID641101

rel-(3R,5S)-3,5-Dimethylpiperidine

C7H15N

结构：O=C(/C=C/c1ccc(CCl)cc1)Nc1ccc(-c2ccc(Cl)cc2)cc1
HCID68816418

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H]1C[C@H](C)CN(Cc2ccc(/C=C/C(=O)Nc3ccc(-c4ccc(Cl)cc4)cc3)cc2)C1
HCID57845848

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 1.2.c. from (E)-N-(4′-chlorobiphenyl-4-yl)-3-(4-chloromethylphenyl)acrylamide and cis-3,5-dimethylpiperidine. Yield: 30 mg (30% of theory); melting point: 217° C.-218° C.; C29H31ClN2O (M=459.03); calc.: molecular ion peak (M+H)+: 459/461; found: molecular ion peak (M+H)+: 459/461.

WORKUP

后处理

  1. customPrepared analogously to Example 1.2.c