HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl(6-nitroquinolin-2-yl)amine → N2-Isopropylquinoline-2,6-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl(6-nitroquinolin-2-yl)amine | HCID 43450861 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | N2-Isopropylquinoline-2,6-diamine | HCID 43450828 | — |
Reaction Steps
Prepared analogously to Example 3.1.b. from isopropyl-(6-nitroquinolin-2-yl)amine. Yield: 0.51 g (78.1% of theory); C12H15N3 (M=201.27); calc.: molecular ion peak (M+H)+: 202; found: molecular ion peak (M+H)+: 202; Rf value: 0.25 (silica gel, dichloromethane/methanol (19:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-0196d0acd1fd41d2b76949c9fa432a48 |
| Source note | uspto-grants-2009_09 |