Sodium 6-(4-fluorophenyl)naphthalene-2-sulfinate → HCID 87616591, compound

Participants

Reaction Steps

Prepared according to the method of Example 6, Step 4 using (1E)-1-(2-iodophenyl)ethanone O-methyloxime and sodium 6-(4-fluorophenyl)naphthalene-2-sulfinate. 1H NMR (400 MHz, d6-DMSO): δ 8.56 (1H, s), 8.35 (1H, s), 8.29-8.27 (2H, m), 8.17 (1H, d, J=8.8 Hz), 8.02 (1H, dd, J=1.7, 8.6 Hz), 7.91 (2H, dd, J=5.5, 8.8 Hz), 7.83-7.71 (3H, m), 7.44 (1H, dd, J=1.7, 7.4 Hz), 7.37 (2H, t, J=8.8 Hz), 3.56 (3H, s), 2.14 (3H, s); m/z (ES+) 434 [MH+].

Provenance & Evidence