HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 10458247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 4-[2-[[7,8-dihydro-8,8-dimethyl-5-(4-methylphenyl)-2-naphthalenyl]seleno]ethynyl]-2-fluorobenzoate | HCID 86601149 | — |
| Product | HCID 10458247 | HCID 10458247 | — |
Reaction Steps
In a manner similar to that of Example 7d, by reacting 1.28 g (2.5 mmol) of methyl 4-(8,8-dimethyl-5-p-tolyl-7,8-dihydro-2-naphthylselanylethynyl)-2-fluorobenzoate with 0.51 g (13 mmol) of sodium hydroxide, a yellow solid is obtained (0.77 g; yield=63%; m.p.=145° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592478B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-bdf0c8acb3d9432eb47da929020ce2cc |
| Source note | uspto-grants-2009_09 |