HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Butadiene → HCID 68816620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Butadiene | HCID 7845 | — |
| Reactant | Ethyl aluminium dichloride | HCID 16686341 | — |
| Reactant | HCID 23103012 | HCID 23103012 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68816620 | HCID 68816620 | — |
Reaction Steps
Prepared according to the general procedure # I, with the following quantities: 4-Ethyl-2-methyl-2-cyclohexen-1-one (27.6 g, 0.20 mol), Butadiene (21.6 g, 0.040 mol), Ethyl aluminium dichloride (1 molar solution in hexane, 100 ml, 0.10 mol), Dichloromethane (300 ml)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592492B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-012df96005084fa0a7dd3f88c28e9755 |
| Source note | uspto-grants-2009_09 |