HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → N-(3-iodophenyl)morpholine-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 1-Iodo-3-isocyanatobenzene | HCID 4499000 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | N-(3-iodophenyl)morpholine-4-carboxamide | HCID 34669033 | — |
Reaction Steps
A solution of 3-iodophenylisocyanate (0.1 g, 0.41 mmol) and morpholine (0.04 mL, 0.45 mmol) in 2 mL dioxane were heated at 100° C. overnight. The solvent was evaporated and the resulting product was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592363B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-2ac11e4619694d1fb29660e57b04f049 |
| Source note | uspto-grants-2009_09 |