HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 57842865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 4-(4-Boronophenyl)butanoic acid | HCID 57842598 | — |
| Reactant | 4-(3-Benzyloxycarbonyl-propoxy)-phenylboronic acid | HCID 57842668 | — |
| Product | HCID 57842865 | HCID 57842865 | 69% |
Reaction Steps
Using a procedure analogous to that used to prepare 1B, 2B (212 mg, 1:1 mixture of 2B and 2A) was reacted with benzyl bromide to afford 2C (90 mg, 69%) as a white solid. 1H NMR (400 MHz, CDCl3) δ 1.92 (m, 2H), 2.33 (t, J=7.0 Hz, 2H), 2.62 (t, 2H), 5.08 (s, 2H), 7.11 (d, 2H), 7.25-7.35 (m, 5H), 7.69 (d, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d632fe29b5b24a96aeaaec4267b90ff2 |
| Source note | uspto-grants-2009_09 |