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HRID735504

反应详情

EQUATION

反应方程式

HRID 735504 的结构方程式

REACTANTS

反应物

3
结构：CC1(C)COB(B2OCC(C)(C)CO2)OC1
HCID2734316

Bis(neopentyl glycolato)diboron

C10H20B2O4

结构：CCS(=O)(=O)c1ccc(NC(=O)CCCc2ccc(Br)cc2C)cc1C#N
HCID57842660

未命名化合物

结构：CC1(C)COB(c2ccc(CCCC(=O)O)cc2)OC1
HCID57842777

未命名化合物

PRODUCTS

生成物

1
结构：CCS(=O)(=O)c1ccc(NC(=O)CCCc2ccc(B3OCC(C)(C)CO3)cc2C)cc1C#N
HCID57842912

未命名化合物

收率 88%

PROCEDURE

实验过程

Using a procedure analogous to that used to prepare 2A, 8B (448 mg, 1.00 mmol) was reacted with 5,5,5′,5′-Tetramethyl-[2,2′]bi[[1,3,2]dioxaborinanyl] to afford 8C (425 mg, 88%) as an off-white solid. MS (ESI) m/z 413.1 (M−H)− for free boronic acid.