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HRID735508

反应详情

EQUATION

反应方程式

HRID 735508 的结构方程式

REACTANTS

反应物

3
结构：O=C(Cl)CCCc1ccc(Br)cc1
HCID246776

4-(4-bromophenyl)butanoyl chloride

C10H10BrClO

结构：CC(C)S(=O)(=O)c1ccc(N)cc1C#N
HCID57448207

5-Amino-2-(propane-2-sulfonyl)benzonitrile

C10H12N2O2S

结构：CCS(=O)(=O)c1ccc(NC(=O)CCCc2ccc(Br)cc2C)cc1C#N
HCID57842660

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)S(=O)(=O)c1ccc(NC(=O)CCCc2ccc(Br)cc2)cc1C#N
HCID57842772

未命名化合物

收率 92%

PROCEDURE

实验过程

Using a procedure analogous to that used to prepare 8B, 9B (364 mg, 1.62 mmol) was reacted with 4-(4-bromophenyl)butyric acid chloride to give 9C (667 mg, 92%). MS (ESI) m/z 449.1, 451.1 (M+H)+.