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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 735562Generated: October 30, 2026

HCID 57842902, compound → HCID 57842775, compound

https://huagongshe.com/reaction/735562

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57842902HCID 57842902—
CatalystNickelHCID 935—
SolventMethanolHCID 887—
ProductHCID 57842775HCID 5784277573%

Reaction Steps

A solution of 25D (460 mg, 0.59 mmol) in MeOH (50 mL) with catalytic Raney Ni was stirred under an atmosphere of H2 (70 psi) for 20 h. The reaction mixture was filtered through Celite and concentrated to give 25E (340 mg, 73%) as a yellow oil. MS (ESI) m/z 790.95 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07592331B2
Source datasetuspto-grants-2009_09
ORD IDord-1f99dc189eb04cf0bf9244b1e5e57af3
Source noteuspto-grants-2009_09