HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57842780, compound → HCID 57842589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57842780 | HCID 57842780 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 57842589 | HCID 57842589 | 99% |
Reaction Steps
A solution of 28E (265 mg, 0.39 mmol) and Pd/C (10%, 40 mg) was stirred under H2 (1 atm) for 15 h. The reaction was filtered through Celite and concentrated to yield 28F (126 mg, 99%) as a yellow oil. MS (ESI) m/z 328.29 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-40523e5dc0b44e14a78a7c7632463bba |
| Source note | uspto-grants-2009_09 |