HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Bromo-2,6-dimethylphenyl)ethanol → HCID 57842545, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Bromo-2,6-dimethylphenyl)ethanol | HCID 57842702 | — |
| Reactant | 4-Bromo-2-methylphenethyl 3-cyano-4-(ethylsulfonyl)phenylcarbamate | HCID 57842863 | — |
| Reactant | HCID 68818495 | HCID 68818495 | — |
| Product | HCID 57842545 | HCID 57842545 | 59% |
Reaction Steps
Using a procedure analogous to that used to prepare 31A, 32B (400 mg, 1.75 mmol) was reacted with 25A (579 mg, 1.75 mmol) to give 32C (480 mg, 59%) as a white solid. MS (ESI) m/z 465.1/467.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d60a2931795b4741a689d1c773fe0b0b |
| Source note | uspto-grants-2009_09 |