HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57842704, compound → 4-(2-(3-((Tert-butoxycarbonylamino)methyl)phenylcarbamoyloxy)ethyl)-3-chlorophenylbromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57842704 | HCID 57842704 | — |
| Reactant | 2-(4-Bromo-2-chlorophenyl)ethan-1-ol | HCID 57842802 | — |
| Reactant | Tert-butyl 3-isocyanatobenzylcarbamate | HCID 83382972 | — |
| Product | 4-(2-(3-((Tert-butoxycarbonylamino)methyl)phenylcarbamoyloxy)ethyl)-3-chlorophenylbromide | HCID 57842553 | 50% |
Reaction Steps
Using a procedure analogous to that used to prepare 34D, 61C (1.94 g, 8.73 mmol) was reacted with 61B to give 61D (1.84 g, 50%) as an oil. MS (ESI) m/z 385.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-9e478959c7b44657a75039201bd966c5 |
| Source note | uspto-grants-2009_09 |