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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 735691Generated: October 31, 2026

4-Bromo-beta,beta-dimethylbenzeneethanol → (2-(4-Bromophenyl)-2-methylpropoxy)(tert-butyl)dimethylsilane

https://huagongshe.com/reaction/735691

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Bromo-beta,beta-dimethylbenzeneethanolHCID 12805124—
Reactant(2-(4-Bromophenyl)propoxy)(tert-butyl)dimethylsilaneHCID 57842594—
Product(2-(4-Bromophenyl)-2-methylpropoxy)(tert-butyl)dimethylsilaneHCID 21986021—

Reaction Steps

According to the procedure for the preparation of 73C, 74A (1.93 g, 8.42 mmol) afforded 3.04 g of 74B as a colorless oil. MS (ESI) m/z 211.1 (M-OTBS)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07592331B2
Source datasetuspto-grants-2009_09
ORD IDord-2d7e1408c35a4f0a98f257de251af046
Source noteuspto-grants-2009_09