HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Bromophenyl)propan-2-ol → (1-(4-Bromophenyl)propan-2-yloxy)(tert-butyl)dimethylsilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Bromophenyl)propan-2-ol | HCID 19882901 | — |
| Reactant | (2-(4-Bromophenyl)propoxy)(tert-butyl)dimethylsilane | HCID 57842594 | — |
| Product | (1-(4-Bromophenyl)propan-2-yloxy)(tert-butyl)dimethylsilane | HCID 57842700 | 87% |
Reaction Steps
According to the procedure for the preparation of 73C, 77A (4.90 g, 22.8 mmol) afforded 6.51 g (87%) of 77B as a colorless oil. MS (ESI) m/z 197.1 (M-OTBS)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-01eb1626c1574e15a6d8f69e5abc13ac |
| Source note | uspto-grants-2009_09 |