HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tridecanoic acid → Ethyl{benzyl[4-(tridecanoylamino)benzyl]amino}(oxo)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tridecanoic acid | HCID 12530 | — |
| Reactant | Ethyl[(4-aminobenzyl)(benzyl)amino](oxo)acetate | HCID 67187687 | — |
| Product | Ethyl{benzyl[4-(tridecanoylamino)benzyl]amino}(oxo)acetate | HCID 67188066 | 39% |
Reaction Steps
The same procedure as employed in the preparation of Example 5, step d using ethyl[(4-aminobenzyl)(benzyl)amino](oxo)acetate and tridecanoic acid gave the title compound as a colorless oil (39%). M−(ESI): 507.2. HPLC (Condition A), Rt: 7 min (HPLC purity-91.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-deeadb137ac349a3977693e2dd5608ca |
| Source note | uspto-grants-2009_09 |