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HRID735825

反应详情

EQUATION

反应方程式

HRID 735825 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCCCCCCCC(=O)O
HCID12530

Tridecanoic acid

C13H26O2

结构：CCOC(=O)C(=O)N(Cc1ccccc1)Cc1ccc(N)cc1
HCID67187687

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCC(=O)Nc1ccc(CN(Cc2ccccc2)C(=O)C(=O)OCC)cc1
HCID67188066

未命名化合物

收率 39%

PROCEDURE

实验过程

The same procedure as employed in the preparation of Example 5, step d using ethyl[(4-aminobenzyl)(benzyl)amino](oxo)acetate and tridecanoic acid gave the title compound as a colorless oil (39%). M−(ESI): 507.2. HPLC (Condition A), Rt: 7 min (HPLC purity-91.3%).

WORKUP

后处理

  1. customThe same procedure as employed in the preparation of Example 5, step d