HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10218354, compound → HCID 69000180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10218354 | HCID 10218354 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69000180 | HCID 69000180 | 54% |
Reaction Steps
The same procedure as employed in the preparation of Example 1 (step c) but using {(4-{[4-(heptyloxy)phenyl]ethynyl}benzyl)[4-(trifluoromethyl)benzyl]amino}(oxo)acetic acid in EtOAc gave the title compound as a colorless oil (54%). M−(LC/MS(ESI)): 554. HPLC (Condition A), Rt: 5.95 min (HPLC purity: 95.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-0f2ed558afcf413e802a6bfd5b64785e |
| Source note | uspto-grants-2009_09 |