HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67186027, compound → HCID 67189385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67186027 | HCID 67186027 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67189385 | HCID 67189385 | 49% |
Reaction Steps
The same procedure as employed in the preparation of Example 1 (step c) but using oxo{(4-{[4-(pentyloxy)phenyl]ethynyl}benzyl)[4-(trifluoromethyl)benzyl]amino}acetic acid in EtOAc gave the title compound as a yellow oil (49%). M−(LC/MS(ESI)): 526. HPLC (Condition A), Rt: 5.62 min (HPLC purity: 74.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b856c4e3bcf14b88a681a0452f310356 |
| Source note | uspto-grants-2009_09 |