HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67188790, compound → HCID 67187743, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67188790 | HCID 67188790 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67187743 | HCID 67187743 | 20% |
Reaction Steps
The same procedure as employed in the preparation of Example 1 (step c) but using 11-[4-({(carboxycarbonyl)[4-(trifluoromethyl)benzyl]amino}methyl)phenyl]undec-10-ynoic acid in EtOAc gave the title compound as a colorless oil (20%). M−(LC/MS(ESI)): 520. HPLC (Condition A), Rt: 5.03 min (HPLC purity: 96.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b022ea2687554e32bca61d6c2020bfe6 |
| Source note | uspto-grants-2009_09 |