HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)benzylamine → N-[3-(trifluoromethyl)benzyl]-N-[3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzyl]amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)benzylamine | HCID 75962 | — |
| Reactant | 3-(3-Undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde | HCID 86598538 | — |
| Product | N-[3-(trifluoromethyl)benzyl]-N-[3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzyl]amine | HCID 67187099 | — |
Reaction Steps
The same procedure as employed in the preparation of Example 357 (step a) but using 3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde and 3-(trifluoromethyl)benzylamine gave the title compound as an oil. M+(LC/MS(ESI)): 488.5. HPLC (Condition A), Rt: 4.86 min (HPLC purity: 66.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-db3438f35f77467e9d412181579a60fa |
| Source note | uspto-grants-2009_09 |