HRID735979

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID67188273

未命名化合物

HCID86598538

未命名化合物

PRODUCTS

生成物

结构：CCCCCCCCCCCc1noc(-c2cccc(CNCc3ccc(S(=O)(=O)C(F)(F)F)cc3)c2)n1

HCID67187372

未命名化合物

PROCEDURE

实验过程

The same procedure as employed in the preparation of Example 357 (step a) but using 3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde and 4-[(trifluoromethyl)sulfonyl]benzylamine hydrochloride gave the title compound as an oil. M+(LC/MS(ESI)): 552.5. HPLC (Condition A), Rt: 4.85 min (HPLC purity: 62.0%).

WORKUP

后处理

customThe same procedure as employed in the preparation of Example 357 (step a) but

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-54e7d93f6fe8481fb72ae4490b396842
来源数据集: uspto-grants-2009_09
DOI: 10.6084/m9.figshare.5104873.v1
专利: US07592477B2
来源说明: uspto-grants-2009_09

反应 SMILES

[CH2:1]([C:12]1[N:16]=[C:15]([C:17]2[CH:18]=[C:19]([CH:22]=[CH:23][CH:24]=2)[CH:20]=O)[O:14][N:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].Cl.[F:26][C:27]([F:40])([F:39])[S:28]([C:31]1[CH:38]=[CH:37][C:34]([CH2:35][NH2:36])=[CH:33][CH:32]=1)(=[O:30])=[O:29]>>[F:39][C:27]([F:26])([F:40])[S:28]([C:31]1[CH:38]=[CH:37][C:34]([CH2:35][NH:36][CH2:20][C:19]2[CH:22]=[CH:23][CH:24]=[C:17]([C:15]3[O:14][N:13]=[C:12]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[N:16]=3)[CH:18]=2)=[CH:33][CH:32]=1)(=[O:29])=[O:30]